Gas chromatograph is a kind of instrument used to detect the residual solvent of packaging printing. It is a professional instrument used to detect the purity and content of solvents. When using gas chromatograph, you may encounter problems with abnormal detector signals. These abnormalities may be caused by a variety of factors, including equipment failure, operating errors, or sample problems. Solving these problems usually requires systematic inspection and elimination of possible causes.
1. Check the detector connection and settings:
- Make sure the detector is properly connected to the chromatograph and all cables and interfaces are not damaged.
- Check the detector setting parameters, such as temperature, gas flow, etc., to ensure that they meet the requirements of the analytical method.
2. Check the gas supply:
- Verify that the flow and pressure of the carrier gas and auxiliary gas are normal.
- Check the gas purification system, such as moisture and oxygen traps, to ensure that they are not saturated or failed.
3. Check the sample injection:
- Make sure the sample has been injected correctly and the injection volume is appropriate.
- Check whether the syringe is contaminated or damaged, and clean or replace it if necessary.
4. Check the chromatographic column:
- Confirm that the chromatographic column is installed correctly and there is no leakage.
- Check if the column is aged or damaged. If so, consider replacing it with a new one.
5. Check the detector status:
- If a flame ionization detector (FID) is used, check if the flame is lit and stable.
- If a thermal conductivity detector (TCD) is used, check if the tungsten filament is intact.
- For other types of detectors, such as a mass spectrometer (MS), check the status of the ion source and electron multiplier.
6. Software and data processing:
- Make sure that the chromatography data system software is installed correctly and there are no errors or conflicts.
- Check baseline noise and drift, and adjust the sensitivity and integration parameters of the detector.
7. Daily maintenance and preventive measures:
- Clean and maintain the detector regularly to maintain its performance.
- Use high-quality gases and reagents to avoid introducing impurities and contaminants.
8. Troubleshooting steps:
- If there is no signal from the detector, first check if the detector is turned on and connected correctly.
- If the signal is weak or there is interference, check the quality of the sample and the column, as well as the sensitivity setting of the detector.
- If the signal is unstable, check the gas supply and the temperature control of the detector.