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Causes of Abnormal Signals in Gas Chromatograph Detector
Time:15.05.2024

Gas chromatograph is a kind of instrument used to detect the residual solvent of packaging printing. It is a professional instrument used to detect the purity and content of solvents. When using gas chromatograph, you may encounter problems with abnormal detector signals. These abnormalities may be caused by a variety of factors, including equipment failure, operating errors, or sample problems. Solving these problems usually requires systematic inspection and elimination of possible causes.

1. Check the detector connection and settings:

- Make sure the detector is properly connected to the chromatograph and all cables and interfaces are not damaged.

- Check the detector setting parameters, such as temperature, gas flow, etc., to ensure that they meet the requirements of the analytical method.

2. Check the gas supply:

- Verify that the flow and pressure of the carrier gas and auxiliary gas are normal.

- Check the gas purification system, such as moisture and oxygen traps, to ensure that they are not saturated or failed.

3. Check the sample injection:

- Make sure the sample has been injected correctly and the injection volume is appropriate.

- Check whether the syringe is contaminated or damaged, and clean or replace it if necessary.

4. Check the chromatographic column:

- Confirm that the chromatographic column is installed correctly and there is no leakage.

- Check if the column is aged or damaged. If so, consider replacing it with a new one.

5. Check the detector status:

- If a flame ionization detector (FID) is used, check if the flame is lit and stable.

- If a thermal conductivity detector (TCD) is used, check if the tungsten filament is intact.

- For other types of detectors, such as a mass spectrometer (MS), check the status of the ion source and electron multiplier.

6. Software and data processing:

- Make sure that the chromatography data system software is installed correctly and there are no errors or conflicts.

- Check baseline noise and drift, and adjust the sensitivity and integration parameters of the detector.

7. Daily maintenance and preventive measures:

- Clean and maintain the detector regularly to maintain its performance.

- Use high-quality gases and reagents to avoid introducing impurities and contaminants.

8. Troubleshooting steps:

- If there is no signal from the detector, first check if the detector is turned on and connected correctly.

- If the signal is weak or there is interference, check the quality of the sample and the column, as well as the sensitivity setting of the detector.

- If the signal is unstable, check the gas supply and the temperature control of the detector.

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